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Beilstein J. Org. Chem. 2012, 8, 371–378, doi:10.3762/bjoc.8.40
Graphical Abstract
Scheme 1: Diketonato metallomesogens and diketones with mesomorphic properties.
Scheme 2: Malonates and cyanoacetates tethered to calamitic 4-cyanobiphenyl units.
Scheme 3: Synthesis of malonate and cyanoacetates tethered to 4-cyano-biphenyl moieties.
Figure 1: DSC traces of 13a (heating/cooling rate 5 K/min).
Figure 2: DSC traces of 11a (heating/cooling rate 10 K/min).
Figure 3: Schlieren textures of 11a and 11b under crossed polarizers, upon cooling (cooling rate 5 K/min) fro...
Figure 4: Schlieren textures of 13a and 13b under crossed polarizers upon cooling (cooling rate 5 K/min) from...
Figure 5: 2D X-ray scattering patterns of 11a: (A) crystalline phase at 50 °C, (B) isotropic phase at 25 °C, ...